Appendix N Information about Chemistry Laboratory-SMC, USST

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Appendix N Information about Chemistry Laboratory

Author：Views：Time：2021-11-15

1. Introduction of chemistry laboratories for chemical experiments.

Room No.

Laboratory

Course

Room area (m²)

406

Chemical Engineering Principle Laboratory

Experiment of Chemical Engineering Principle

502

Analysis Chemistry

Laboratory

Analytical Chemistry Experiment

110

503

Instrumental Analysis Laboratory

Instrumental Analysis Experiment

504

General Chemistry Laboratory

General Chemistry Experiment

112

505

Inorganic Chemistry Laboratory

Inorganic Chemistry Experiment

106

509

Comprehensive Laboratory

Comprehensive Experiment

601

Biochemistry Laboratory

Engineering Biochemistry Experiment

67.2

602

Physical Chemistry Laboratory

Physical Chemistry Experiment

120

617

Organic Chemistry

Laboratory

Organic Chemistry Experiment

120

Equipment, administrator, opening time and rules for each of the laboratory (listed above)

Room 406	Chemical Engineering Principle Laboratory
1. Equipment	Description
View
Experimental device for determining characteristic curve of centrifugal pump	Familiar with the various pipe fittings and valves that make up the pipeline, understand the temperature, pressure, electric power, flow and other on-site display instruments and sensing detection equipment, and master the measurement principle and use method of the turbine flowmeter.
Sieve plate tower rectification experiment device	Determine the total theoretical plate number, total plate efficiency and single plate efficiency of the distillation column after stable operation under the condition of total reflux. Determine the number of theoretical plates, total plate efficiency and single plate efficiency of the rectification column after stable operation under a certain reflux ratio.
Chemical heat transfer comprehensive experimental device	Through the experimental research on the air-steam simple double-pipe heat exchanger, master the method of measuring the convective heat transfer coefficient, and deepen the understanding of its concept and influencing factors
Experimental device for measuring fluid flow resistance	Learn how to measure the frictional resistance of straight pipes △Pf and the friction coefficient of straight pipes λ; Grasp the relationship between the friction coefficient λ and the Reynolds number Re under different flow rates and the law of change. Verify the relationship between λ and Re in the laminar, transitional, and turbulent regions; Determine the local drag coefficient x when the fluid flows through the valve in a turbulent state;
Tower gas absorption experiment device	Understand the principle and effect of purifying SO in exhaust gas by absorption method. Change the speed of the empty tower and observe the gas-liquid contact status and flooding phenomenon in the packed tower. Master the method of measuring the absorption efficiency and pressure reduction of the packed absorption tower.
Decompression reactor	The inner layer can be filled with reaction materials for stirring reaction, and the interlayer can be passed through different cold and heat sources (refrigerant, hot water and hot oil) for cyclic heating or cooling reactions. Under the set constant temperature condition, the sealed glass reactor can carry out constant-rate and constant-rate stirring reaction under normal pressure or negative pressure according to the requirements of use, and can carry out the reflux and distillation of the reaction solution.
2. Administrator	One Associate Professor and two lab technicians
3. Opening time	8:00-17:00 (Monday to Friday)
4. Main Experiments	☑ Determining Characteristic Curve of Centrifugal Pump ☑ Sieve plate tower rectification experiment ☑ Chemical heat transfer comprehensive experiment ☑ Measuring fluid flow resistance ☑ Tower gas absorption experiment
5. Rules	The laboratory can be used by both teachers and students under the supervision of working staff

Experimental Science Center Room 502	Analytic chemistry Laboratory
1. Equipment	Description
View
4 experiment tables with ventilating system and 3 fume hoods	It was designed for students to conducting experiments safely.
30 sets of electric heating-jackets	30 sets of electric heating-jackets to heat the solution in beakers.
30 sets of glassware toolboxes, burettes and related iron stands	30 sets of glassware toolbox, burettes and related iron stand for basic experiments.
8 analytical balances	8 analytical balances to weigh samples.
1 oven	1 oven to dry glassware or metalware.
1 set of water purification machine	1 set of water purification machine to provide pure water for experiments.
2 sets of ultrasonic cleaners	2 sets of ultrasonic cleaners to clean glassware.
4 sets of water-cycling pumps	4 sets of water-cycling pumps to provide vacuum for sucking filtration.
1 set of ice machine	1 set of ice machine to provide ice for common cooling purposes
2. Administrator	One Associate Professor and two lab technicians
3. Opening time	8:00-17:00 (Monday to Friday)
4. Main Experiments	☑Preparation and concentration comparison of acid and base standard solution ☑Calibration of acid and base standard solution ☑Determination of NaOH and Na₂CO₃ in mixed alkali sample ☑Determination of molar mass of organic acids ☑Determination of acetic acid in edible vinegar ☑Determination of calcium carbonate in eggshells ☑Additivity test of absorbance ☑The Determination of trace Cr (VI) and Mn (VII) in water at the same time ☑Preparation and calibration of EDTA standard solution ☑Determination of calcium and magnesium ion content and total hardness of water ☑Preparation and calibration of sodium thiosulfate standard solution ☑Determination of glucose content (indirect iodimetry) ☑Determination of iron content by phenanthroline spectrophotometry ☑Determination of sulfur in soluble sulfates
5. Rules	The laboratory can be used by both teachers and students under the supervision of working staff

Room 503	Instrumental Analysis Laboratory
1. Equipment	Description
1 set of UV-Vis Spectrophotometer	UV/V spectroscopy is routinely used in analytical chemistry for the quantitative determination of different analytes, such as transition metal ions, highly conjugated organic compounds, and biological macromolecules. Spectroscopic analysis is commonly carried out in solutions but solids and gases may also be studied. 1 set of TU-1901 Double Beam UV-Vis Spectrophotometer. 1 computer.
1 set of Electrochemical Workstation	Studies the relationship between electricity; These reactions involve electric charges moving between electrodes and an electrolyte (or ionic species in a solution). 1 Chenhua Electrochemical Workstation. 1 computer.
1 set of Atomic Absorption Spectrometer	Atomic absorption spectroscopy (AAS) is a spectroanalytical procedure for the quantitative determination of chemical elements using the absorption of optical radiation (light) by free atoms in the gaseous state. Atomic absorption spectroscopy is based on absorption of light by free metallic ions. 1 set of TAS-990AFG Atomic Absorption Spectrometer. 1 computer.
1 set of Liquid Chromatography	Liquid Chromatography is a laboratory technique for the separation of a mixture. Analytical chromatography is done normally with smaller amounts of material and is for establishing the presence or measuring the relative 1 set of Agilent Technologies 1200Series Liquid Chromatography. 1 computer.
1 set of Gas Chromstograpgy	Gas chromatograph is an instrument for qualitative and quantitative analysis of multi-component complex mixtures using chromatographic separation and detection techniques. 1 set of PERSEE G5 Gas Chromstograpgy 1 computer
1 set of Fluorescence Spectrometer	Fluorescence spectroscopy is a type of electromagnetic spectroscopy that analyzes fluorescence from a sample. It involves using a beam of light, usually ultraviolet light, that excites the electrons in molecules of certain compounds 1 set of RF-5301PC SHIMADZU Fluorescence Spectrometer 1 computer
1 set of Fourier Transform Infrared Spectroscopy	Fourier-transform infrared spectroscopy (FTIR) is a technique used to obtain an infrared spectrum of absorption or emission of a solid, liquid or gas. An FTIR spectrometer simultaneously collects high-resolution spectral data over a wide spectral range. 1 set of Thermo NICOLET 380 Fourier Transform Infrared Spectroscopy 1 computer
1 set of Ion meter	Ion meter is an electrochemical analytical instrument used to measure ion concentration in solution 1set of METTLER TOLEDO Ion meter 1 computer
2. Administrator	Two Associate Professor and two lab technicians
3. Opening time	8:00-17:00 (Monday to Friday)
4. Main Experiments	☑ Determination of phenol trichlorophenol by dual wavelength ultraviolet spectrum ☑ Electrochemical voltammetry (determination of electrode reaction of potassium ferricyanide) ☑ Determination of iron and copper in soybean milk by atomic absorption spectrometry ☑ Analysis of caffeine in tea cola by liquid chromatography ☑ Determination of alcohol content in wine samples by gas chromatography ☑ Determination of vitamin B2 by fluorescence spectrophotometry ☑ Infrared spectroscopy (KBr tablet method for identification of sodium benzoate) ☑Determination of F- in natural water by ion selective electrode method
5. Rules	The laboratory can be used by both teachers and students under the supervision of working staff

Room 504	Organic Chemistry Laboratory
1. Equipment	Description
View
3 experiment tables with ventilating system and 2 fume hoods	It was designed for students to conducting experiments safely.
SEM：Observe the microscopic morphology of materials
8 electronic balance	To measure the mass of chemicals
5 thermostat water bath	HH-S6 Thermostat water bath for heating up the chemicals
pH meter	PHS-3C pH meter for measuring the pH value of solution
D.C. regulated power supply	QJ3005H D.C. regulated power supply for specific current and voltage
Ultra-pure water system	UPT-I-10T Ultra-pure water system for deionized water
Conductivity meter	DDS-307A Conductivity meter for measuring the conductivity of solution
Spectrophotometer	722 Spectrophotometer for measuring the absorbance of solution
Glass apparatus	Common glassware for various purposes like synthesis\extraction\ column chromatography purification\titration\ volumetric weighing etc
Isothermal magnetic stirrer	20 DF-101S Isothermal magnetic stirrer for heating and mixing the solution.
2. Administrator	One senior experimentalist and three experimentalists
3. Opening time	8:00-17:00 (Monday to Friday)
4. Main Experiments	☑ code of practice and common glassware practice ☑ determination of ionization constant of acetic acid ☑ determination of iron content by absorbance spectrophotometry ☑ galvanizing by electricity ☑ water quality testing ☑ oscillation reaction - iodine-bell reaction
5. Rules	The laboratory can be used by both teachers and students under the supervision of working staff

Room 505	Inorganic Chemistry Laboratory
1. Equipment	Description
View
Central exhaust system	Central exhaust system for air conditioning in the lab
8 analytical balance	To measure the mass of chemicals
Thermostat water bath	HH-S6 Thermostat water bath for heating up the chemicals
pH meter	PS-1C pH meter for measuring the pH value of solution
Spectrophotometer	722 Spectrophotometer for measuring the absorbance of solution
glass apparatus	Common glassware for various purposes like synthesis\extraction\ column chromatography purification\titration\ volumetric weighing etc
4 water-cycling pump	4 pumps to provide vacuum for sucking filtration
30 sets of Electric Constant temperature heating heating-jackets	Heating sleeves equipped with temperature sensors;
2. Administrator	One senior experimentalist and three experimentalists
3. Opening time	8:00-17:00 (Monday to Friday)
4. Main Experiments	☑ Code of practice and common glassware practice ☑ Determination of the equilibrium constant of acetic acid dissociation ☑ Determination of chemical equilibrium constants by absorbance spectrophotometry ☑ galvanizing by electricity ☑ water quality testing ☑ oscillation reaction - iodine-bell reaction ☑ Anionic cation identification ☑ Preparation of ammonium ferrous sulfate ☑ Preparation of Hexaamminecobalt(III) chloride ☑ Preparation of copper sulfate and determination of crystal water ☑ Preparation of potassium trioxalate and ferrite ☑ The burning iron
5. Rules	The laboratory can be used by both teachers and students under the supervision of working staff

Experimental Science Center Room 509	Comprehensive Chemistry Laboratory
1. Equipment	Description
View
2 fume hoods for conducting experimental organic chemistry	Each fume hood (170 75 80 cm) was designed for one student to conducting organic chemistry experiments safely and independently
6 heating stirrer, glassware toolbox and related iron stand	6 heating stirrers equipped with temperature sensors; Common glassware for various purposes like synthesis\extraction\ column chromatography purification\titration\ volumetric weighing etc.
2 Oven and thermostat water bath	2 ovens to dry glassware， 1 thermostat water bath to heat liquids.
1 tripurpose ultraviolet analyzer	1 tripurpose ultraviolet analyzer for checking the quality of hormone alkaloids, vitamins and other drugs that can produce fluorescence.
1 roto evaporator	1 roto evaporator for removing solvents from the mixture
1 water-cycling pump	1 pump to provide vacuum for sucking filtration
1 henghui DC power supply	1 DC power supply station for testing the stability of synthesized materials.
1 electrochemical station	1 electrochemical station and 1 xenon lamp steady current supply for testing the electrochemical performances such as LSV, CV, EIS and so on.
2. Administrator	One Associate Professor and two lab technicians
3. Opening time	8:00-17:00 (Monday to Friday)
4. Main Experiments	☑ Laboratory safety education ☑ Preparation of pearlescent Shampoo ☑ Preparation of polyurethane foam plastics ☑ Preparation of sunscreen and determination of sunscreen index ☑ Hydrothermal synthesis of titanium dioxide ☑ Extraction of caffeine from tea
5. Rules	The laboratory can be used by both teachers and students under the supervision of working staff

Room 601	Biochemistry Laboratory
1. Equipment	Description
1 set of fume hood	1 set of fume hood was designed for safely solution preparation and organic chemistry experiments
20 sets of intelligent digital display multifunctional oil bath pot	Heating stirrers equipped with temperature sensors;
2 ovens	1 common oven to dry samples or glassware 1 vacuum oven to dry samples containing a small amount of water under vacuum conditions
1set of water-cycling pump	1set of pump to provide vacuum for sucking filtration
1set of ultrapure water machine	Used for preparing distilled water and deionized water
1 set of water molecular titrator	Rapid determination of moisture content in samples
pH/conductivity meter	The conductivity or pH of a rapid liquid sample
20 alcohol lamps	20 alcohol lamps
2. Administrator	Two lecturers
3. Opening time	8:00-17:00 (Monday to Friday)
4. Main Experiments	☑ The separation of amino acids by plate chromatography ☑ The determination of amylase activity ☑ Protein content was determined by coomassie bright blue G-250 method ☑ The preparation of culture medium ☑ Soil dilution, separation, purification and aseptic operation techniques. ☑ The simple staining of bacteria and gram staining ☑ The usage of microscopes and the observation of microbial specimens
5. Rules	The laboratory can be used by both teachers and students under the supervision of working staff

Room 602	Physical Chemistry Laboratory
1. Equipment	Description
1 set of electrochemical analyzer	Used for the measurement of electrochemical data, including: 1 electrochemical workstation 1 computer 1 set of electrodes including platinum electrode, calomel electrode, glassy carbon electrode
1 set of microcoulomb comprehensive analyzer	Used for the analysis of sulfur, chlorine, nitrogen in samples, including 1 computer 1 set of microcoulomb comprehensive analyzer
1 set of automatic polarimeter	Use for measuring the rotation of materials. The measurement results can be automatically converted by PC, and the concentration, content and purity of the samples can be analyzed.
1 set of thermogravimetric analyzer	Use for measuring the relationship between temperature and mass change, including: 1 computer 1 set of thermogravimetric analyzer
1 set of Brunauer-Emmett-Teller	Used for measuring specific surface area of materials, including 3 roto evaporators for removing solvents from the mixture 1 computer
1 set of heat of combustion analyzer	Used for measuring the heat of combustion, including 1 set of heat of combustion analyzer 1 computer
1 set of digital abbe refractometer	It is an analytical instrument used to measure the refractive index in the field of biology.

2. Administrator	Two Professor and one lab technicians
3. Opening time	8:00-17:00 (Monday to Friday)
4. Main Experiments	☑ Determination of the gross heat of combustion ☑ Thermogravimetric analysis ☑ The measurement of specific surface area ☑ The phase diagram of completely mutually soluble two-liquid system ☑ The equilibrium constant of liquid phase reaction ☑ Determination of partial molar volume of solution ☑ Determination of electromotive force and its application ☑ Conversion of sucrose ☑ Saponification reaction of ethyl acetate ☑ Determination of surface tension of solution ☑ The control of temperature ☑ Determination of solution viscosity
5. Rules	The laboratory can be used by both teachers and students under the supervision of working staff

Room 617	Organic Chemistry Laboratory
1. Equipment	Description
View
20 fume hoods for conducting experimental organic chemistry	Each fume hood (170 75 80 cm) was designed for one student to conducting organic chemistry experiments safely and independently
40 heating stirrer, glassware toolbox and related iron stand	40 heating stirrers equipped with temperature sensors; Common glassware for various purposes like synthesis\extraction\ column chromatography purification\titration\ volumetric weighing etc
1 Oven	To dry glassware，metalware when needed
3 roto evaporators	3 roto evaporators for removing solvents from the mixture
10 water-cycling pumps	10 pumps to provide vacuum for sucking filtration
1 ice machine	1 set of ice machine to preparation of ice for common cooling purposes
3 sets of recirculating chillers	3 sets of recirculating chillers to provide low temperature (-78 °C) for some synthetic reactions or other special purposes
Digital melting-point apparatus	Type WRS-1B for the determination of melting points of organic compound
Automatic Polarimeter	WZZ-2S Automatic Polarimeter for determination of enantiopure organic compounds
2. Administrator	One Associate Professor and two lab technicians
3. Opening time	8:00-17:00 (Monday to Friday)
4. Main Experiments	☑ Asprin Synthesis ☑ Recrystallization of benzoic acid ☑ Synthesis of 2-chlorobutane ☑ Purification by column chromatography ☑ Resolution of α-phenylethylamine ☑ Extraction of caffeine from tea ☑ Synthesis of sulfonamide antibiotics ☑ Synthesis of ethyl benzoate ☑Synthesis of 3-methyl acetophenone
5. Rules	The laboratory can be used by both teachers and students under the supervision of working staff

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